Graph with corresponding diffraction pattern in Figure 1c. As expected, the microstructure (each SEM and TEM) is featureless and amorphous in nature, as confirmed by the hollow ring inside the diffraction pattern (Figure 1c). Furthermore, the BMG is homogeneous in nature and there’s no existence of any defects, like the porosities and also the cavities. The EDX spectrum, as shown in Figure 1d, shows the presence of all constituent PX-478 Epigenetic Reader Domain components except beryllium (Be). The amount of Be in the material was out with the detection range of the EDX. three.2. In Situ Compression of Micro-Pillars Fabricated micro-pillars around the polished BMG samples are shown in Figure two. Figure 2a shows an array of representative micro-pillars that had been fabricated within the middle of a 30 crater, with each other using a higher magnification image of different diameter micro-pillars in Figure 2b . The typical diameter of the micro-pillars is as follows: 3.1 0.05 , 4.05 0.06 and 4.98 0.05 . The micro-pillars within this study are somewhat tapered (two ) in nature, which was not possible to avoid as a result of material-ion beam interaction [27]. For the duration of in situ compression, load-displacement curves had been logged inside the pc technique, which have been then converted into tension train curves, in accordance with the technique explained in Section two.three. To demonstrate the impact of strain price and pillar diameter on strain train behaviour, the curves had been aggregated into two distinct groups. Figure three exhibits the effect of pillar diameter on a provided strain rate, whereas Figure four exhibits the impact of strain price on a provided pillar diameter.-Irofulven custom synthesis Metals 2021, 11, 1611 Metals 2021, 11, x FOR PEER REVIEW4 of 15 4 of(d)Figure 1. Microstructure of presently investigated Zr-based BMG: (a) SEM micrograph, (b) TEM micrograph, (c) diffraction pattern and (d) corresponding EDX spectra. Pt denotes platinum that was deposited to defend the material surface in the course of TEM sample preparation in FIB-SEM.3.two. In Situ Compression of Micro-Pillars Fabricated micro-pillars around the polished BMG samples are shown in Figure 2. Figure 2a shows an array of representative micro-pillars that have been fabricated inside the middle of a 30 crater, together with a higher magnification image of distinctive diameter micro-pillars Figure 1. Microstructure of presently investigated Zr-based BMG: (a) SEM micrograph, (b) TEM micrograph, diffraction Figure 1. Microstructure of presently investigated Zr-based BMG: (a) SEM micrograph, (b) TEM micrograph, (c) (c) diffracin Figure 2b . The typical diameter tion pattern and (d) corresponding spectra. Pt denotes platinum that in the micro-pillars is as follows: three.1 urface in 4.05 the material 0.05 , pattern and (d) corresponding EDXEDX spectra. Pt denotes platinum that was deposited to safeguard material surface inside the was deposited to safeguard 0.06 in FIB-SEM.0.05 . The micro-pillars within this studythe somewhat tapered (two and four.98 are the course of TEM sample preparation course of TEM sample preparation in FIB-SEM. in nature, which was not probable to prevent because of material-ion beam interaction [27]. 3.2. In Situ Compression of Micro-Pillars Fabricated micro-pillars on the polished BMG samples are shown in Figure two. Figure 2a shows an array of representative micro-pillars that had been fabricated within the middle of a 30 crater, with each other having a higher magnification image of distinctive diameter micro-pillars in Figure 2b . The average diameter in the micro-pillars is as follows: three.1 0.05 , four.05 0.06 and four.98 0.
